An in-situ TEM investigation of He bubble evolution in SiC

نویسندگان

  • C J Pawley
  • M F Beaufort
  • E Oliviero
  • J A Hinks
  • J F Barbot
  • S E Donnelly
چکیده

This paper presents work using the capabilities of two TEM with in-situ ion irradiation facilities: Microscope and Ion Accelerator for Materials Investigation (MIAMI) at the University of Huddersfield and Joint Accelerators for Nano-science and Nuclear Simulation JANNuS at Centre de Spectrométrie Nucléaire et de Spectrométrie de Masse (CSNSM), Orsay, France, to study the nucleation and growth of He bubbles in silicon carbide (SiC) and to carry out an investigation into bubble behaviour at high temperatures and under displacing irradiation. Preliminary results on bubble nucleation and growth during He irradiation of SiC are presented together with results from a simultaneous anneal and highenergy heavy-ion irradiation of samples containing He bubbles. The displacing irradiation is observed to impede He bubble growth resulting in smaller bubbles than those obtained from an anneal alone. A tentative interpretation of these observations is presented.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

In situ Observation of Microstructure Evolution in 4H-SiC under 3.5keV He Irradiation

4H-SiC was irradiated with 3.5 keV He ions using the MIAMI facility at University of Huddersfield. The evolution of microstructure and gas bubbles during the irradiation at 700°C, 800°C and 900°C was observed by in situ transmission electron microscopy. Under irradiation, isolated bubbles and bubble discs formed in the SiC matrix. Bubble discs lying on {0001} and {10-10} crystal planes were beg...

متن کامل

Investigation of the effect of sample volume on the synthesis of B4C / SiC nanocomposite powder by mechanical activation volume combustion synthesis method assisted by spark plasma instrument

In this study, B4C / SiC nanocomposite powder with 1 to 1 molar ratio was synthesized completely in situ, with high purity and at low temperature by mechanical activation volume combustion synthesis method. At first, raw materials consist of B2O3, Mg, C and Si were weighed. The weighed materials were mixed and milled for 9 hours by planetary ball mil and under argon atmosphere. Milled materials...

متن کامل

Helium bubble formation in nuclear glass by in-situ TEM investigations

The effect of helium implantation fluences in French nuclear borosilicate glass on He bubble nucleation and growth mechanisms was characterised using in-situ TEM experiments. Observations of implanted glass at 143K indicate that a helium concentration of around 3 at.% is required to nucleate a significant density of nanosized bubbles. He bubble growth is observed for He concentration higher tha...

متن کامل

Evolution of Helium Bubbles and Discs in Irradiated 6H-SiC during Post-Implantation Annealing

The single crystal 6H-SiC with [0001] crystal direction irradiated by 400 keV He⁺ ions with 1 × 1017 ions/cm² fluence at 400 °C were annealed at 600, 900, 1200 and 1400 °C for different durations. The evolution of helium bubbles and discs was investigated by transmission electron microscopy. An irradiated layer distributed with fine helium bubbles was formed with a width of ~170 nm after helium...

متن کامل

In situ activation of a Ni catalyst with Mo ion for hydrogen evolution reaction in alkaline solution

In this study Ni catalyst have been activated during hydrogen evolution reaction (HER) by adding Mo ions into the alkaline electrolyte. After dissolving different amounts of ammonium molybdate in the 1M NaOH as electrolyte, Ni catalyst was used as cathode for HER. Afterwards a comparison between hydrogen overpotential measured in Ni catalyst with and without in situ activation has been made; th...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2015